No 3 (2023)

Cover Page

The profile physical coefficient and its application for modelling the machined surface texture

Bobrovskij I.N.

Abstract

Current trends in the development of mechanical engineering impose increasingly stringent requirements for the performance characteristics of manufactured goods. The main parameters characterizing the quality of a product as a whole are the physical, mechanical, and geometric indicators of the working surfaces of the compound units. In domestic practice, a machined surface is mainly characterized by a rather limited number of parameters (no more than 6), such as the average microroughness height, the microroughness height at 10 points, etc. However, their use is not enough to manufacture competitive products in the modern conditions. For example, international ISO/ASME/DIN standards include a much broader set of parameters required to accurately describe the performance properties of a surface. The paper analyzes the approaches to the formation of requirements for the microgeometry of the working surfaces of parts used in modern mechanical engineering. Based on the analysis, the author proposed and mathematically substantiated a general approach to modelling surface texture characteristics, which allows describing adequately the surface using a new parameter – the profile physical coefficient, since it is virtually impossible to directly compare the technologies developed in Russia with foreign analogues based on the current standards. First, the profile physical coefficient was determined at the section level. Next, it was decomposed into a Fourier series for the two-dimensional and three-dimensional cases. The paper presents the analysis of the new parameter applicability on the example of a product obtained by honing. The author concluded about the applicability of this parameter and the necessity to develop a comprehensive methodology based on it for evaluating the surface after machining.

Frontier Materials & Technologies. 2023;(3):9-17
pages 9-17 views

Development and airworthiness certification of state of art additively manufactured AlSi10Mg mission critical selector valve body part for aerospace

Vignesh P., Praveen K., Krishnakumar S., Bhuvaneswari M., Kale S., Ram Prabhu T.

Abstract

Aerospace applications can benefit from additive manufacturing (AM), which is highly advantageous for prototyping and rapid manufacturing. It also offers cost and weight savings, as well as integrated design capabilities. As of now, there are only a few AM standards available, many materials and equipment are involved, resulting in many variables that hinder certification and adoption. As a result, nonstandard testing is making AM in the airborne materials less appealing due to its costly and time-consuming nature. The main objective of this work is to manufacture the Selector Valve Body parts of military and civil aircraft through Laser Powder Bed Fusion (LPBF) process using AlSi10Mg powder. Further, this paper has been carried out the metallurgical properties, non-destructive and destructive testing as well as the clear explanation about the certification procedures. Moreover, this underscores the need for the developing guidelines, and standards that cover all aspects of manufacturing from design to manufacturing to operation. A comprehensive analysis from liquid penetration test shows defects are within the permissible level. In addition, it exhibits higher yield strength, ultimate strength, and elongation of (259±4) MPa, (323±4) MPa, and (12.5±1.5) % respectively, along with factual evidence that the precipitation hardened AlSi10Mg indigenously developed and produced is equal in properties to the equivalent precipitation hardening aluminium alloys produced by internationally renowned manufacturers. 

Frontier Materials & Technologies. 2023;(3):19-30
pages 19-30 views

Simulation of contact thermal resistance when designing processing equipment

Denisenko A.F., Podkruglyak L.Y.

Abstract

Analysis of the processing equipment structures when designing according to the temperature criterion is a necessary guarantee of ensuring the required performance characteristics. The presence of a significant number of parts in the processing equipment units and mechanisms requires, when designing, the prediction of the heat flow passage through the joints. When simulating contact thermal resistance, the variety of requirements for a joint can be taken into account by introducing a pseudolayer into the contact zone. The paper presents test results of the proposed regression dependence of the temperature change when the heat flow goes through the pseudolayer obtained considering four significant factors: the pseudolayer thickness, the nominal pressure, the material yield strength, and the actual contact zone location. The adequacy of the specified regression dependence was verified experimentally and applying numerical simulation using large-block finite elements. To describe the process of heat transfer in the thermal model elements, the authors determined contact thermal resistances for several conditions for the heat flow propagation: from one finite element to another within one part; from one finite element to another located in an adjacent part; heat flow passing through closed cavities; heat flow propagation into the environment for finite elements located on the outer (free) contour of the part. The experiments showed a good agreement between the experimental data and the simulation results. The application of large-block finite elements based on the proposed contact thermal resistance model allowed bringing the FE simulation technique to engineering use without complex software.

Frontier Materials & Technologies. 2023;(3):31-42
pages 31-42 views

Control of the dynamic stability of metal-cutting systems in the process of cutting based on the fractality of roughness of the machined surface

Kabaldin Y.G., Sablin P.A., Schetinin V.S.

Abstract

The problem of increasing the efficiency of mechanical treatment within modern automated production is relevant for many branches of the processing industry. This problem requires a deep study of the physical processes occurring during cutting. The urgency of the problem increases even more with the development of digital production in our country. Today, in the presence of a wide range of products, enterprises are forced to create conditions for reducing the technological cycle when manufacturing a particular product. To carry out the study, an experiment was conducted in which the U8 carbon steel was used as the processed material, and the T15K6 alloy was used as the tool material. During the experiment, the authors observed a change in the roughness of the machined surface depending on the cutting speed. The paper considers the possibility of assessing the quality of the surface layer during cutting based on fractal and neural network modeling. It is identified that the fractal dimension shows the regularity of the reproduction of the machined surface roughness during cutting. The calculated fractal dimension of the machined surface roughness correlates well with the values of the machined surface roughness (correlation coefficient is 0.8–0.9). A neural network structure has been developed, which allows controlling the machined surface quality depending on the cutting conditions. The authors studied the possibility of using neural network models to control technological systems of cutting treatment. When creating digital twins, it is proposed to take into account factors affecting the quality of the treated surface and processing performance, which are poorly accounted for in modeling, as well as when conducting full-scale experiments during machining. Such factors are wear of the cutting tool, the process of plastic deformation, and cutting dynamics.

Frontier Materials & Technologies. 2023;(3):43-51
pages 43-51 views

The influence of the supply mains parameters on the stability of phase control during resistance welding

Klimov A.S., Kudinov A.K., Klimov V.S., Eltsov V.V., Boldyrev D.A.

Abstract

Resistance welding in large-scale manufacturing is carried out with a significant number of disturbances, the cumulative effect of which may exceed the capabilities of modern control equipment. Most resistance welding control systems used in industry to compensate for existing disturbances provide welding current phase control depending on the measured parameters characterizing the process of welded joint formation. The efficiency of such controllers is largely determined by the accuracy of measuring and setting the phase control parameters, which include the opening and conduction angles of welding thyristors. The paper shows that when switching on a contact machine, a phase shift of the mains voltage occurs in the load mode relative to the mains voltage in the idle mode. Using a simplified electric equivalent circuit of a contact welding machine, the paper describes the nature of the phase shift of the mains voltage. Circuit active resistance and inductance are selected as parasitic parameters of the mains. The authors simulated the electrical processes in the contact machine according to the three-loop equivalent circuit. The study shows the influence of mains parasitic parameters on the phase regulation stability, the features of the obtained current and voltage oscillograms. Depending on the mains and contact welding machine parameters, the phase shift magnitude ranges from fractions to units of an electrical degree. With welding current parametric stabilization by the mains voltage, the influence of mains parasitic parameters can be neglected. When the regulator operates in the mode of maintaining the secondary current numerical value, a decrease in the generated current relative to the specified one is observed. The authors proposed and tested a technique for determining the parasitic parameters of the supply mains based on the results of a short circuit test.

Frontier Materials & Technologies. 2023;(3):53-60
pages 53-60 views

Formation of a bimetallic Ti–Al material by a wire-feed electron-beam additive manufacturing

Luchin A.V., Astafurova E.G., Astafurov S.V., Reunova K.A., Zagibalova E.A., Kolubaev E.A.

Abstract

Currently, there is a request from aerospace and aircraft for the construction materials with sufficiently high mechanical strength, thermal creep, corrosion and oxidation resistance. The conventional alloys used for these purposes are too heavy. At the same time, alternative light materials such as Ti–Al-based alloys have many flaws, when they are produced by conventional methods. This work considers the possibility to produce the Ti–Al-based alloys by the method of a wire-feed electron-beam additive manufacturing (EBAM). We study the chemical and phase compositions, microstructure and microhardness of a bimetallic Ti–Al alloy, obtained by this method. It is found the formation of five characteristic regions between titanium and aluminum parts of the bimetallic billet. The mixing zone consists of TiAl and TiAl3 intermetallics, that is confirmed by the investigation of microstructure, chemical and phase compositions. According to XRD (X-ray diffraction) and EDS (energy-dispersive X-ray spectroscopy) analyses, it can be assumed that TiAl intermetallic prevails over TiAl3 one. The average microhardness of the mixing zone equals to 450 HV (≈4.4 GPa). This zone has developed dendritic microstructure, and even distribution of the phases without link to dendritic and inter-dendritic zones. The cracks appearing in this area are filled with the material of the upper layers, so the whole material is poreless and defect-free. Thus, the results of this work have shown a fundamental possibility to produce the intermetallic Ti–Al alloys with the use of the EBAM.

Frontier Materials & Technologies. 2023;(3):61-70
pages 61-70 views

The effect of strain rate on mechanical properties and fracture mode of the AZ31 alloy and commercially pure magnesium pre-exposed in a corrosive medium

Merson E.D., Poluyanov V.A., Myagkikh P.N., Merson D.L.

Abstract

Magnesium alloys are promising materials for aviation, automotive engineering, and medicine, however, due to the low resistance to stress corrosion cracking (SCC), their wide application is limited. To create alloys with high resistance to SCC, a comprehensive study of this phenomenon nature is required. Previously, it was suggested that diffusible hydrogen and corrosion products formed on the magnesium surface can play an important role in the SCC mechanism. However, the contribution of each of these factors to the SCC-induced embrittlement of magnesium and its alloys is understudied. Since the influence of diffusible hydrogen on the mechanical properties of metals increases with the strain rate decrease, the study of the strain rate sensitivity of the SCC-susceptibility of magnesium alloys is a critical task. In this work, the authors studied the effect of the strain rate in the range from 5·10−6 to 5·10−4 s−1 on the mechanical properties, the state of the side and fracture surfaces of the as-cast commercially pure magnesium and the AZ31 alloy before and after exposure to a corrosive environment and after removal of corrosion products. The study identified that the preliminary exposure to a corrosive medium leads to the AZ31 alloy embrittlement, but does not affect the mechanical properties and the fracture mode of pure magnesium. The authors found that the AZ31 alloy embrittlement caused by the preliminary exposure to a corrosive medium appears extensively only at the low strain rate and only if the layer of corrosion products is present on the specimens’ surface. The study shows that a change in the strain rate has little effect on the mechanical properties of pure magnesium. The authors concluded that the main cause of the AZ31 alloy embrittlement after soaking in a corrosive medium is the corrosion products layer, which presumably contains the embrittling agents such as hydrogen and residual corrosive medium.

Frontier Materials & Technologies. 2023;(3):71-82
pages 71-82 views

The kinetics of L10 superstructure formation in the Cu–56Au alloy (at. %): resistometric study

Podgorbunskaya P.O., Zgibnev D.A., Gavrilova A.A., Novikova O.S., Volkov A.Y.

Abstract

Due to the improved strength properties compared to the equiatomic Cu–50 at. % Au alloy, non-stoichiometric Cu–56 at. % Au alloy can be used both in dentistry and as a corrosion-resistant conductor of weak electrical signals in tool engineering. The work studies the kinetics of the disorder→order phase transformation in the Cu–56Au alloy, during which the disordered fcc lattice (A1-phase) is rearranged into an atomically ordered one with the L10 superstructure. The initial disordered state of the alloy was obtained in two ways: applying plastic deformation by 90 % or quenching at a temperature of above 600 °C (i. e., from the region of the A1-phase existence). To form the L10 superstructure, annealing was carried out at temperatures of 200, 225, and 250 °C. The annealing duration ranged from 1 h to 2 months. Resistometry was chosen as the main technique to study the kinetics of the disorder→order transformation. The temperature dependences of the electrical resistivity of the alloy in various structural states are obtained. The authors constructed the graphs of the electrical resistance dependence on the annealing time logarithm, based on which, the rate of the new phase formation was estimated. To evaluate the structural state of the alloy at various transformation stages, the authors used X-ray diffraction analysis (XRD). The crystal structure rearrangement during the transformation is shown by the example of splitting the initial cubic A1-phase peak (200) into two tetragonal ordered L10 phase peaks – (200) and (002). Based on the resistometry and X-ray diffraction analysis data, the authors carried out a quantitative assessment of the rate of the disorder→order phase transformation in the alloy under the study. It is established that the values of the converted volume fraction (resistometry) and the long-range order degree (X-ray diffraction analysis) are close. The study shows that in the temperature range of 200–250 °C, the rate of atomic ordering according to the L10 type in the nonstoichiometric alloy Cu–56 at. % Au is maximum at 250 °C. It is identified that the disorder→order transformation in the initially quenched specimens of the investigated alloy proceeds approximately an order of magnitude faster than in preliminarily deformed specimens.

Frontier Materials & Technologies. 2023;(3):83-94
pages 83-94 views

Determination of the volume fraction of primary carbides in the microstructure of composite coatings using semantic segmentation

Soboleva N.N., Mushnikov A.N.

Abstract

In the process of formation of composite coatings, partial dissolution of strengthening particles (most often carbides) in the matrix is possible; therefore, in some cases, the material creation mode is chosen taking into account the volume fraction of primary carbides not dissolved during coating deposition. The methods currently widely used for calculating the volume fraction of carbides in the structure of composite coatings (manual point method and programs implementing classical computer vision methods) have limitations in terms of the possibility of automation. It is expected that performing semantic segmentation using convolutional neural networks will improve both the performance of the process and the accuracy of carbide detection. In the work, multiclass semantic segmentation was carried out including the classification on the image of pores and areas that are not a microstructure. The authors used two neural networks based on DeepLab-v3 trained with different loss functions (IoU Loss and Dice Loss). The initial data were images of various sizes from electron and optical microscopes, with spherical and angular carbides darker and lighter than the matrix, in some cases with pores and areas not related to the microstructure. The paper presents mask images consisting of four classes, created manually and by two trained neural networks. The study shows that the networks recognize pores, areas not related to the microstructure, and perfectly segment spherical carbides in images, regardless of their color relative to the matrix and the presence of pores in the structure. The authors compared the proportion of carbides in the microstructure of coatings determined by two neural networks and a manual point method.

Frontier Materials & Technologies. 2023;(3):95-102
pages 95-102 views

Concerning the selection of areas with a dominant type of dependence when analyzing production control data

Timoshenko V.V., Budanova E.S., Kodirov D.F., Sokolovskaya E.A., Kudrya A.V.

Abstract

The formation of representative databases determines the interest in forecasting and managing the quality of metal based on data mining using special software products often based on regression analysis and not always taking into account the statistical nature of an object of study itself. This can lead to misinterpretation of the results or incomplete extracted information reducing the efficiency of statistical processing. Based on the analysis of the production database of the technology for producing 13G1S-U sheet steel, the authors evaluated the possibilities of multiple linear regression for predicting the quality of a steel sheet. The study shows that the type of distribution of the values of control parameters, the distribution nature of which was estimated based on the determination of the skewness and kurtosis coefficients, limits the regression forecast depth. Due to the great deviation of the predicted models from the experimental values in the right tail area of the distribution of the impact strength values, in this work, the authors developed the methods for separating data arrays and proposed criteria to compare the obtained results. To assess the accuracy of the results obtained, arrays with a deliberately asymmetric distribution were selected from the initial sample, against which the statistical characteristics were also compared. Based on the proposed techniques, the authors identified the dominant chemical elements that contribute to the difference in the distribution of the values of acceptance properties existing within the same standard technology. The study shows that the proposed separation method can be used as a variation of cognitive graphics techniques to identify areas with a dependence dominant type based on the correlation of skewness and kurtosis coefficients.

Frontier Materials & Technologies. 2023;(3):103-114
pages 103-114 views

Features of microstructure formation in the AK4-1 and AK12D aluminum alloys after their joint friction stir processing

Khalikova G.R., Basyrova R.A., Trifonov V.G.

Abstract

Friction stir processing is one of the modern methods of local modification of the surface of aluminum alloys in the solid-phase state, which provides the dispersion of structural components. In heat-hardened aluminum alloys with a matrix type structure, heat treatment following after friction stir processing can lead to abnormal grain growth in the stir zone. However, in alloys with the structure close to microduplex type, a fine-grained structure can be formed after friction stir processing and heat treatment. This work is aimed at evaluating the possibility of increasing the microstructure thermal stability of the AK4-1 (Al–Cu–Mg–Fe–Si–Ni) matrix-type aluminum alloy. For this purpose, AK12D (Al–Si–Cu–Ni–Mg) aluminum alloy with the structure close to microduplex type was locally mixed into the studied alloy by friction stir processing. Subsequent Т6 heat treatment was carried out according to the standard mode for the AK4-1 alloy. Studies showed that the stir zone had an elliptical shape with an onion-ring structure. This structure comprised alternating rings with different amounts and sizes of excess phases. At the same time, in the stir zone center, the width of rings and the average area of excess phases were larger compared to the stir zone periphery, where the width of rings and the average area of particles were smaller. The average area of excess phases in the rings with their higher content was smaller than in the rings with their lower content. This distribution of excess phases leads to the formation of a fine-grained microstructure, where the average size of grains depends on the interparticle distance in the α-Al solid solution.

Frontier Materials & Technologies. 2023;(3):115-124
pages 115-124 views

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