Features of microstructure formation in the AK4-1 and AK12D aluminum alloys after their joint friction stir processing

Cover Page

Cite item

Abstract

Friction stir processing is one of the modern methods of local modification of the surface of aluminum alloys in the solid-phase state, which provides the dispersion of structural components. In heat-hardened aluminum alloys with a matrix type structure, heat treatment following after friction stir processing can lead to abnormal grain growth in the stir zone. However, in alloys with the structure close to microduplex type, a fine-grained structure can be formed after friction stir processing and heat treatment. This work is aimed at evaluating the possibility of increasing the microstructure thermal stability of the AK4-1 (Al–Cu–Mg–Fe–Si–Ni) matrix-type aluminum alloy. For this purpose, AK12D (Al–Si–Cu–Ni–Mg) aluminum alloy with the structure close to microduplex type was locally mixed into the studied alloy by friction stir processing. Subsequent Т6 heat treatment was carried out according to the standard mode for the AK4-1 alloy. Studies showed that the stir zone had an elliptical shape with an onion-ring structure. This structure comprised alternating rings with different amounts and sizes of excess phases. At the same time, in the stir zone center, the width of rings and the average area of excess phases were larger compared to the stir zone periphery, where the width of rings and the average area of particles were smaller. The average area of excess phases in the rings with their higher content was smaller than in the rings with their lower content. This distribution of excess phases leads to the formation of a fine-grained microstructure, where the average size of grains depends on the interparticle distance in the α-Al solid solution.

About the authors

Gulnara R. Khalikova

Institute for Metals Superplasticity Problems of RAS, Ufa;
Ufa State Petroleum Technological University, Ufa

Author for correspondence.
Email: gulnara.r.khalikova@gmail.com
ORCID iD: 0000-0002-6712-8469

PhD (Engineering), senior researcher, assistant professor of Chair “Technological Machines and Equipment”, assistant professor of Chair “Metal Technology in Oil-and-Gas Mechanical Engineering”

Russian Federation

Regina A. Basyrova

Institute for Metals Superplasticity Problems of RAS, Ufa

Email: regina1296@yandex.ru

research assistant

Russian Federation

Vadim G. Trifonov

Institute for Metals Superplasticity Problems of RAS, Ufa;
Ufa State Petroleum Technological University, Ufa

Email: vadimt@imsp.ru
ORCID iD: 0000-0002-8187-1355

PhD (Engineering), leading researcher, assistant professor of Chair “Metal Technology in Oil-and-Gas Mechanical Engineering”

Russian Federation

References

  1. Zykova A.P., Tarasov S.Yu., Chumaevskiy A.V., Kolubaev E.A. A Review of friction stir processing of structural metallic materials: process, properties, and methods. Metals, 2020, vol. 10, no. 6, article number 772. doi: 10.3390/met10060772.
  2. Mishra R.S., Ma Z.Y. Friction stir welding and processing. Materials Science and Engineering: R: Reports, 2005, vol. 50, no. 1-2, pp. 1–78. doi: 10.1016/j.mser.2005.07.001.
  3. Mirian Mehrian S.S., Rahsepar M., Khodabakhshi F., Gerlich A.P. Effects of friction stir processing on the microstructure, mechanical and corrosion behaviors of an aluminum-magnesium alloy. Surface and Coatings Technology, 2021, vol. 405, article number 126647. doi: 10.1016/j.surfcoat.2020.126647.
  4. Croteau J.R., Jung J.G., Whalen S.A. et al. Ultrafine-grained Al–Mg–Zr alloy processed by shear-assisted extrusion with high thermal stability. Scripta Materialia, 2020, vol. 186, pp. 326–330. doi: 10.1016/j.scriptamat.2020.05.051.
  5. He Ch., Li Y., Wei J., Zhang Zh., Tian N., Qin G., Zhao X. Enhancing the mechanical performance of Al–Zn–Mg alloy builds fabricated via underwater friction stir additive manufacturing and post-processing aging. Journal of Materials Science and Technology, 2022, vol. 108, pp. 26–36. doi: 10.1016/j.jmst.2021.08.050.
  6. Belov N.A. Fazovyy sostav promyshlennykh i perspektivnykh alyuminievykh splavov [Phase Composition of Industrial and Prospective Aluminium Alloys]. Moscow, MISiS Publ., 2010. 511 p.
  7. Heidarzadeh A., Mironov S., Kaibyshev R. et al. Friction stir welding/processing of metals and alloys: a comprehensive review on microstructural evolution. Progress in Materials Science, 2021, vol. 117, article number 100752. doi: 10.1016/j.pmatsci.2020.100752.
  8. Feng X., Liu H., Lippold J.C. Microstructure characterization of the stir zone of submerged friction stir processed aluminum alloy 2219. Materials Characterization, 2013, vol. 82, pp. 97–102. doi: 10.1016/j.matchar.2013.05.010.
  9. Rhodes C.G., Mahoney M.W., Bingel W.H., Spurling R.A., Bampton C.C. Effects of friction stir welding on microstructure of 7075 aluminum. Scripta Materialia, 1997, vol. 36, no. 1, pp. 69–75. doi: 10.1016/S1359-6462(96)00344-2.
  10. Fonda R.W., Bingert J.F. Microstructural evolution in the heat-affected zone of a friction stir weld. Metallurgical and Materials Transactions A, 2004, vol. 35, pp. 1487–1499. doi: 10.1007/s11661-004-0257-7.
  11. Qin H., Zhang H., Wu H. The evolution of precipitation and microstructure in friction stir welded 2195-T8 Al–Li alloy. Materials Science and Engineering: A, 2015, vol. 626, pp. 322–329. doi: 10.1016/j.msea.2014.12.026.
  12. Zuiko I.S., Mironov S., Betsofen S., Kaibyshev R. Suppression of abnormal grain growth in friction-stir welded Al–Cu–Mg alloy by lowering of welding temperature. Scripta Materialia, 2021, vol. 196, article number 113765. doi: 10.1016/j.scriptamat.2021.113765.
  13. Charit I., Mishra R.S. Abnormal grain growth in friction stir processed alloys. Scripta Materialia, 2008, vol. 58, pp. 367–371. doi: 10.1016/j.scriptamat.2007.09.052.
  14. Kalinenko A., Vysotskiy I., Malopheyev S., Mironov S., Kaibyshev R. New insight into the phenomenon of the abnormal grain growth in friction-stir welded aluminum. Materials Letters, 2021, vol. 302, article number 130407. doi: 10.1016/j.matlet.2021.130407.
  15. Khodabakhshi F., Simchi A., Kokabi A.H., Gerlich A.P., Nosko M. Effects of post-annealing on the microstructure and mechanical properties of friction stir processed Al–Mg–TiO2 nanocomposites. Materials and Design, 2014, vol. 63, pp. 30–41. doi: 10.1016/j.matdes.2014.05.065.
  16. Humphreys F.J. A unified theory of recovery, recrystallization and grain growth, based on the stability and growth of cellular microstructures – I. The basic model. Acta Materialia, 1997, vol. 45, no. 10, pp. 4231–4240. doi: 10.1016/S1359-6454(97)00070-0.
  17. Humphreys F.J. A unified theory of recovery, recrystallization and grain growth, based on the stability and growth of cellular microstructures – II. The effect of second-phase particles. Acta Materialia, 1997, vol. 45, no. 12, pp. 5031–5039. doi: 10.1016/S1359-6454(97)00173-0.
  18. Khalikova G.R., Zakirova G.R., Farkhutdinov A.I., Korznikova E.A., Trifonov V.G. Surface hardening of an Al–Si–Cu–Ni–Mg aluminum alloy by friction stir processing and T6 heat treatment. Letters on Materials, 2022, vol. 12, no. 3, pp. 255–260. doi: 10.22226/2410-3535-2022-3-255-260.
  19. Khodabakhshi F., Nosko M., Gerlich A.P. Dynamic restoration and crystallographic texture of a friction-stir processed Al–Mg–SiC surface nanocomposite. Materials Science and Technology, 2018, vol. 34, no. 14, pp. 1773–1791. doi: 10.1080/02670836.2018.1490858.
  20. Ma Z.Y., Sharma S.R., Mishra R.S. Microstructural modification of as-cast Al–Si–Mg alloy by friction stir processing. Metallurgical and Materials Transactions A, 2006, vol. 37, pp. 3323–3336. doi: 10.1007/BF02586167.
  21. Yang J., Wang D., Xiao B.L., Ni D.R., Ma Z.Y. Effects of rotation rates on microstructure, mechanical properties, and fracture behavior of friction stir-welded (FSW) AZ31 magnesium alloy. Metallurgical and Materials Transactions A, 2013, vol. 44, pp. 517–530. doi: 10.1007/s11661-012-1373-4.
  22. Cui G.R., Ma Z.Y., Li S.X. Periodical plastic flow pattern in friction stir processed Al–Mg alloy. Scripta Materialia, 2008, vol. 58, no. 12, pp. 1082–1085. doi: 10.1016/j.scriptamat.2008.02.003.
  23. Andrade D.G., Leitão C., Dialami N., Chiumenti M., Rodrigues D.M. Analysis of contact conditions and its influence on strain rate and temperature in friction stir welding. International Journal of Mechanical Sciences, 2021, vol. 191, article number 106095. doi: 10.1016/j.ijmecsci.2020.106095.
  24. Avettand-Fénoël M.-N., Taillard R., Laye J., Odiévre T. Experimental investigation of three-dimensional (3-D) material flow pattern in thick dissimilar 2050 friction-stir welds. Metallurgical and Materials Transactions A, 2014, vol. 45, pp. 563–578. doi: 10.1007/s11661-013-2015-1.
  25. Schneider J.A., Nunes A.C. Characterization of plastic flow and resulting microtextures in a friction stir weld. Metallurgical and Materials Transactions B, 2004, vol. 35, pp. 777–783. doi: 10.1007/s11663-004-0018-4.
  26. Yang B.C., Yan J.H., Sutton M.A., Reynolds A.P. Banded microstructure in AA2024-T351 and AA2524-T351 aluminum friction stir welds: Part I. Metallurgical studies. Materials Science and Engineering: A, 2004, vol. 364, no. 1-2, pp. 55–65. doi: 10.1016/S0921-5093(03)00532-X.
  27. Zhou Y.Z., Zhang W., Wang B.Q., Guo J.D. Ultrafine-grained microstructure in a Cu–Zn alloy produced by electropulsing treatment. Journal of Materials Research, 2003, vol. 18, pp. 1991–1997. doi: 10.1557/JMR.2003.0276.
  28. Xu S.W., Deng X.M. A study of texture patterns in friction stir welds. Acta Materialia, 2008, vol. 56, no. 6, pp. 1326–1341. doi: 10.1016/j.actamat.2007.11.016.
  29. Ma X., Xu Sh., Wang F., Zhao Y., Meng X., Xie Y., Wan L., Huang Y.Y. Effect of temperature and material flow gradients on mechanical performances of friction stir welded AA6082-T6 joints. Materials, 2022, vol. 15, no. 19, article number 6579. doi: 10.3390/ma15196579.
  30. Woo W., Choo H., Withers P.J., Feng Z. Prediction of hardness minimum locations during natural aging in an aluminum alloy 6061-T6 friction stir weld. Journal of Materials Science, 2009, vol. 44, pp. 6302–6309. doi: 10.1007/s10853-009-3868-y.
  31. Mehdi H., Mishra R.S. Effect of friction stir processing on mechanical properties and heat transfer of TIG welded joint of AA6061 and AA7075. Defence Technology, 2021, vol. 17, no. 3, pp. 715–727. doi: 10.1016/j.dt.2020.04.014.

Supplementary files

Supplementary Files
Action
1. JATS XML

Copyright (c)



This website uses cookies

You consent to our cookies if you continue to use our website.

About Cookies