No 1 (2025)
- Year: 2025
- Published: 31.03.2025
- Articles: 8
- URL: https://vektornaukitech.ru/jour/issue/view/65
-
Description:
Published 31.03.2025
Development of a laboratory tribotechnical facility for testing PDC cutters for wear
Abstract
In the practice of drilling oil and gas wells with diamond bits equipped with PDC cutters, cutter quality non-compliance with the declared class occurs. At the same time, the currently used methods of full-scale testing, when granite stone is used as a counterbody, are time-consuming and expensive, which complicates their use for prompt incoming inspection of new batches of PDC cutters arriving for assembly of diamond bits. This necessitated the development of a laboratory tribotechnical facility for quantitative assessment of the ability of PDC cutters to resist abrasion against abrasive materials. The study covers the development of a specialized tribotechnical facility that allows testing PDC cutters of various sizes for wear during friction against a diamond-containing metal work face, for which it is proposed to use diamond cutting wheels. The developed laboratory tribotechnical facility includes: an electromechanical rotary drive (a drilling-and-milling machine); a measuring unit with sensors for normal loads, friction force and temperature of cutter self-heating during testing; a lever loading mechanism; a set of mandrels for the possibility of installing PDC cutters of various sizes; a data collection system and licensed software. The results of practical evaluation of the developed laboratory tribotechnical facility on PDC cutters of various batches showed that testing on the new equipment allows for quick collection of data on the wear rate of the working edges of PDC cutters. The developed methods, equipment and criteria can be used to certify the wear resistance of PDC cutters.



Structure and mechanical properties of high-entropy alloys of the CoCrZrMnNi system with different Zr and Mn contents produced by vacuum-induction melting
Abstract
The mechanical properties and microstructure of high-entropy alloys (HEA) of the CoCrZrMnNi system produced by vacuum-induction melting are studied depending on the change in the Zr and Mn content. The effect of the Zr and Mn percentage on the microstructure and mechanical properties (Young’s modulus, nanohardness, microhardness) of the high-entropy alloys of the CoCrZrMnNi system is estimated. The relationship between varying the percentage of Zr and Mn and changing the grain size and mechanical properties of high-entropy alloys is studied. The structure, chemical composition and distribution of the intensity of characteristic X-ray radiation of atoms are studied using scanning electron microscopy. The study by scanning electron microscopy methods has demonstrated that in CoCrZrMnNi alloys, with an increase in the zirconium content and a decrease in the manganese content closer to the equiatomic composition, the material structure became more homogeneous. Changing the percentage of zirconium from 8 to 28 at. % contributed to the grain size reduction from 30 to 5 μm and a more uniform elemental distribution. The Сo19.8Cr17.5Zr15.3Mn27.7Ni19.7 alloy demonstrated the highest nanohardness (10 GPa) and Young’s modulus (161 GPa) during instrumental indentation with an indenter load of 50 mN. The Сo20.4Cr18.0Zr7.9Mn33.3Ni20.3 alloy has the lowest nanohardness, Young’s modulus, and microhardness among other alloys, which may be related to the coarse-grained structure with a grain size of up to 30 μm. As the indenter load increased to 5 N, the microhardness of the Сo19.8Cr17.5Zr15.3Mn27.7Ni19.7 alloy decreased compared to the Сo18.7Cr16.5Zr28.9Mn17.4Ni18.6 alloy, which may indicate more universal mechanical properties of alloys with equiatomic zirconium content.



Cutting ceramics for turning of specialised stainless hard-to-machine steel
Abstract
This study shows the possibility of using cutting ceramics as a turning tool. Replaceable standard cutting plates made of VOK-60 and VOK-71 cutting ceramics are used. In the work, based on simulation modelling in the DEFORM software environment, the possibility of high-speed processing with the specified cutting ceramics is substantiated and then experimentally confirmed. Additionally, the authors propose to apply hardening coatings by condensation with ion bombardment, which ensures an increase in the cutting speed to 100 m/min and more with an increase in the service life of the cutting ceramics from 3 to 3.8 times. The maximum stresses in the tool material and the deformation rate of the process material are studied. To select rational solutions in simulation modelling, the authors used the “temperature in the cutting zone”, “stresses in the tool material”, and “tool wear” parameters, which characterise the combined tension of the tool material. The transition from these parameters to the predictive design of cutting ceramics was performed by measuring the cutting force during natural cutting. The measured values of the cutting force components were used to calculate the stresses in the tool material. The study confirmed the hypothesis that the cutting ceramics is capable of operating under the conditions of processing viscous hard-to-machine corrosion-resistant specialised stainless steels such as 09H17N7Yu (C-0.09; Cr-17; Ni-7; Al-1) grade (EU 1.4568, X7CrNiAl17-7), which have a high content of chromium (16–17.5 %) and nickel (7–8 %). The authors propose original technological methods to improve the performance of the cutting ceramics through special heat treatment and coating deposition. In particular, heat treatment in a vacuum at a temperature of 1100–1400 °C for 20–40 min increased the bulk strength of the ceramics, and additional thermochemical treatment by ion nitriding performed at the final stage of heat treatment made it possible to alloy the bond.



The influence of silicon content on the structure of Cu55Ni6Mn4Zn brazing alloy and on the structure and properties of brazed joints
Abstract
Cu55Ni6Mn4Zn (MNMts55-6-4) copper-zinc alloy is widely used for brazing hard-alloy tools and steels. However, the presence of silicon in the alloy (0.1–0.4 wt. %) can lead to the formation of brittle silicides of iron, nickel, and manganese, which negatively influences the strength of brazed joints. The purpose of the study was to determine the influence of the quantitative content of silicon in copper-zinc brazing alloy doped jointly with nickel and manganese on the structure of brazing alloy blanks before brazing and the structure and properties of brazed joints. In the work, to study the distribution of silicides in ingots, tapes, and brazed seams, the authors used microstructural analysis methods, including electron microscopy and X-ray spectral microanalysis. The results showed that with a silicon content of up to 0.2 wt. %, silicides form finely dispersed inclusions uniformly distributed throughout the seam. However, with an increase in the silicon content to 0.4 wt. %, the formation of continuous layers of iron silicides along the brazing alloy – steel boundary is observed, which leads to brittle failure of the joints under mechanical loads. The influence of small gaps turned out to be especially critical during brazing, where the formation of large crystals of iron silicides significantly reduces the strength of the joints. The scientific novelty of the work lies in identifying the optimal silicon content in the alloy (no more than 0.2 wt. %) to minimize the negative effect of silicides on the properties of brazed joints. The results obtained can be used to develop process recommendations for the production of brazing alloys and brazing of steels, which will allow improving the reliability and durability of brazed joints under production-line conditions.



Calculation of the effective solidification range and its relationship with hot brittleness of alloys based on Mg–Al and Mg–Zn systems
Abstract
Magnesium alloys of the Mg–Al and Mg–Zn systems have a wide effective solidification range (ESR), and as a result, have the tendency to hot brittleness during casting. There are several methods for analyzing and calculating the hot brittleness of magnesium alloys, but they are very labor-intensive. In this regard, the objective of the study is to develop a model for calculating the hot brittleness index (HBI) based on the value of the calculated effective solidification range, identifying and analyzing their relationship in binary and multicomponent alloys based on the Mg–Al and Mg–Zn systems. The ESR was calculated using the Thermo-Calc program (TTMG3 database). The ESR was calculated as the difference between the temperature of formation of a given amount of solid phases and the nonequilibrium solidus temperature. The study showed a good correlation between the calculated values of ESR and hot brittleness index in both binary and multicomponent magnesium alloys. In the Mg–Al system alloys, the calculated dependences of the ESR at 90 % of solid phases (ESR90) show the best correlation with the experimental values of HBI. In the binary alloys of the Mg–Zn system, a qualitatively similar dependence is observed. However, no clear correlation was noted between the ESR and HBI. The ESR65 and ESR80 dependences demonstrate the closest nature. According to the relationship between HBI and ESR, the considered multicomponent alloys are divided into two groups as a first approximation: the first one is the Mg–Al–Zn system alloys; the second one is the Mg–Zn–Zr and Mg–Nd–Zr alloys. Within these groups, the dependence of hot brittleness index and ESR has a nature close to a linear one. To describe the dependence of all alloys, a single equation can be applied if ESR65 is used in the calculations for Mg–Al–Zn alloys and ESR90 – for Mg–Zn–Zr and Mg–Nd–Zr alloys. The proposed model will allow for easy and quick calculation of the HBI, which is very important in the development of new high-tech magnesium alloys.



Effect of erbium and hafnium microalloying on the formation of Al3Sc particles in aluminium alloy with a high magnesium content
Abstract
The paper studies the effect of hafnium and erbium additives on the microstructure formation during heat treatment of aluminium alloys with a high magnesium content additionally alloyed with scandium and zirconium. For the study, ingots of aluminium alloys with a high content of magnesium alloyed with scandium, erbium and hafnium with a content in the ranges of 0.03–0.16 % and 0.05–0.16 %, respectively, were produced by casting in a steel chill mould. After casting, the samples were treated with heat at a temperature of 370 and 440 °C with a holding time of 2 to 96 h. Changes in microhardness depending on the heat treatment were studied. For 1590-3 and 1590-4 alloys in the as-cast condition and after heat treatment at a temperature of 440 °C for 2 and 48 h, the fine microstructure and coarse intermetallic compounds were studied using transmission microscopy. The study found that additions of hafnium and erbium lead to an increase in microhardness due to a decrease in the size and an increase in the number of Al3Sc nanoparticles. After heat treatment at a temperature of 440 °C for 4 h, Al3Sc particles of the same size (8 nm) and density precipitate in all the alloys under study. However, with an increase in the holding time in the alloy with a lower hafnium content and a higher erbium content, the particle size increases by 2 times compared to the particles of the alloy where the hafnium content is higher and the erbium content is low.



Influence of crystallographic texture on the strength and electrical conductivity of ultrafine-grained copper
Abstract
The paper covers the study of the influence of equal-channel angular pressing (ECAP) on the structure, crystallographic texture, mechanical properties and electrical conductivity of Cu-ETP copper (Russian analogue – M1), as well as the dependence of these characteristics on the orientation of the measurement direction relative to the cross-section (from −45 to 90°). The specific electrical conductivity and strength characteristics of the material in the as-delivered condition (hot-rolled) and the effect of annealing at a temperature of 450 °C of the original sample are investigated. Mechanical tests for uniaxial tension, a study of microhardness using the Vickers method and a study of specific electrical conductivity based on measuring the parameters of the vortex field excited in the surface layers of the body are carried out. It is found that ECAP processing leads to a significant increase in the ultimate tensile strength to 425 MPa compared to the initial state of 300 MPa. The maximum tensile strength of 425 MPa is achieved at orientation angles relative to the ECAP cross-section of −45°. A significant increase in microhardness to 1364–1405 MPa, tensile strength to 350–425 MPa and electrical conductivity to 101.4–102.4 % IACS is a consequence of the selected directions of cutting the samples relative to the ECAP axis. This indicates the dependence of both mechanical and electrical properties of ultrafine-grained samples on the crystallographic texture orientation. A Cu-ETP copper sample subjected to ECAP with a cutting angle deviating from the ECAP cross-section of the sample by 7.5° has the most optimal crystallographic orientation. In this case, the values of microhardness and electrical conductivity reached 1405 MPa and 102.4 % IACS, respectively.



Mathematical modelling to predict the tensile strength of additively manufactured AlSi10Mg alloy using artificial neural networks
Abstract
Integrating machine learning in additive manufacturing to simulate real manufacturing outcomes can significantly reduce the cost of manufacturing through selective manufacturing. However, limited research exists on developing a prediction model for the mechanical properties of the material. The input variables include key selective laser melting process parameters such as laser power, layer thickness, scan speed, and hatch spacing, with tensile strength as the output. The artificial neural network (ANN) based mathematical model is compared with a second-degree polynomial regression model. The robustness of both models was further assessed with the new data points beyond those used in the development of ANN-based mathematical model and regression model. The results demonstrate that the proposed ANN-based mathematical model offers superior accuracy, with a mean absolute percentage error (MAPE) value of 4.74 % and the R2 (goodness of fit) value of 0.898 in predicting the strength of AlSi10Mg. The ANN-based mathematical method also demonstrates the strong performance on the new data, achieving a regression value of 0.68. This concludes that the model shows sufficient proof to consider a viable option for predicting the tensile strength.


