The study of transformations of supercooled austenite during step quenching of 20Cr2Mn2SiNiMo steel
- Authors: Maisuradze M.V.1, Kuklina A.A.2, Nazarova V.V.1
-
Affiliations:
- Ural Federal University named after the first President of Russia B.N. Yeltsin
- Ural State Mining University Ural Federal University named after the first President of Russia B.N. Yeltsin
- Issue: No 2 (2024)
- Pages: 53-65
- Section: Articles
- URL: https://vektornaukitech.ru/jour/article/view/939
- DOI: https://doi.org/10.18323/2782-4039-2024-2-68-5
- ID: 939
Cite item
Abstract
Currently, step quenching of steels in the temperature range of martensitic transformation, including quenching – partitioning, has found wide application in the automotive industry. Step quenching technology is successfully used to increase a set of properties, which most often include temporary tensile strength and relative elongation. The authors carried out a dilatometric study of the supercooled austenite transformations occurring in the 20Cr2Mn2SiNiMo steel, when implementing various options of step quenching with holding in the martensitic region. It was found that after single-stage quenching, single-stage quenching followed by tempering, and two-stage quenching, primary martensite, isothermal bainite, and secondary martensite are formed in various quantitative ratios. Using X-ray diffraction phase analysis, the amount of residual austenite was determined during step quenching. It has been shown that two-stage quenching makes it possible to stabilise up to 14 % of residual austenite, in the structure of the studied steel, at room temperature. Research has revealed that 20Cr2Mn2SiNiMo steel is characterised by a decrease in the crystal lattice parameter of the residual austenite, with an increase in its content in the steel structure. Uniaxial tensile and impact bending tests were carried out, and the values of the mechanical properties were determined. It has been found that during two-stage quenching, higher strength and elongation values, with lower values of relative contraction and impact strength are achieved compared to oil quenching and low-temperature tempering. The study showed that, with regard to the structural reliability of machine-building parts, step quenching is not the optimal heat treatment mode for the steel under study. The best combination of strength, ductility and impact hardness is achieved after quenching and low-temperature tempering.
About the authors
Mikhail V. Maisuradze
Ural Federal University named after the first President of Russia B.N. Yeltsin
Email: m.v.maisuradze@urfu.ru
ORCID iD: 0000-0003-2850-2988
PhD (Engineering), Associate Professor, assistant professor of Chair “Heat Treatment and Physics of Metals”
Россия, 620002, Russia, Yekaterinburg, Mira Street, 19Aleksandra A. Kuklina
Ural State Mining UniversityUral Federal University named after the first President of Russia B.N. Yeltsin
Author for correspondence.
Email: kuklina@m.ursmu.ru
ORCID iD: 0000-0003-3779-3254
PhD (Engineering), assistant professor of Chair “Physics”, Head of Scientific-Research and Testing Laboratory of Geocryology, Soil Physics and Materials, engineer of Laboratory of Structural Methods of Analysis and Properties of Materials and Nanomaterials
Россия, Address 1: 620144, Russia, Yekaterinburg, Kuibyshev Street, 30. Address 2: 620002, Russia, Yekaterinburg, Mira Street, 19Vera V. Nazarova
Ural Federal University named after the first President of Russia B.N. Yeltsin
Email: kamicure@yandex.ru
postgraduate student of Chair “Heat Treatment and Physics of Metals”
Россия, 620002, Russia, Yekaterinburg, Mira Street, 19References
- Speer J.G. Phase transformations in quenched and partitioned steels. Phase transformations in steels. Diffusionless Transformations, High Strength Steels, Modelling and Advanced Analytical Techniques. Cambridge, Woodhead Publishing Limited, 2012. Vol. 2, pp. 247–270. doi: 10.1533/9780857096111.2.247.
- Liu Xingyu, Han Ying, Wei Junhu, Zu Guoqing, Zhao Yu, Zhu Weiwei, Ran Xu. Effect of tempering temperature on microstructure and mechanical properties of a low carbon bainitic steel treated by quenching-partitioning-tempering (QPT) process. Journal of Materials Research and Technology, 2023, vol. 23, pp. 911–918. doi: 10.1016/j.jmrt.2023.01.061.
- Zahrani M.M., Ketabchi M., Ranjbarnodeh E. Microstructure development and mechanical properties of a C–Mn–Si–Al–Cr cold rolled steel subjected to quenching and partitioning treatment. Journal of Materials Research and Technology, 2023, vol. 22, pp. 2806–2818. doi: 10.1016/j.jmrt.2022.12.130.
- Xu Wen-hua, Li Yang, Xiao Gui-yong, Gu Guo-chao, Lu Yu-peng. Effects of quenching and partitioning on microstructure and properties of high-silicon and high-aluminum medium carbon alloy steels. Materials Today: Communications, 2023, vol. 34, article number 105031. doi: 10.1016/j.mtcomm.2022.105031.
- Tian Yu, Tan Zhunli, Wang Jiong, Zhang Min. Realization of quenching & dynamic partitioning on large-size parts. Materials and Manufacturing Processes, 2022, vol. 37, no. 13, pp. 1490–1499. doi: 10.1080/10426914.2021.2016815.
- Samanta S., Das S., Chakrabarti D., Samajdar I., Singh S.B., Haldar A. Development of multiphase microstructure with bainite, martensite, and retained austenite in a Co-containing steel through quenching and partitioning (Q&P) treatment. Metallurgical and Materials Transactions A, 2013, vol. 44, pp. 5653–5664. doi: 10.1007/s11661-013-1929-y.
- Kumar S., Singh S.B. Evolution of microstructure during the “quenching and partitioning (Q&P)” treatment. Materialia, 2021, vol. 18, article number 101135. doi: 10.1016/j.mtla.2021.101135.
- Zambrano O.A. A Review on the Effect of Impact Toughness and Fracture Toughness on Impact-Abrasion Wear. Journal of Materials Engineering and Performance, 2021, vol. 30, pp. 7101–7116. doi: 10.1007/s11665-021-05960-5.
- Chintha A.R., Valtonen K., Kuokkala V.-T., Kundu S., Peet M.J., Bhadeshia H.K.D.H. Role of fracture toughness in impact-abrasion wear. Wear, 2019, vol. 428-429, pp. 430–437. doi: 10.1016/j.wear.2019.03.028.
- Pang J.C., Li S.X., Wang Z.G., Zhang Z.F. Relations between fatigue strength and other mechanical properties of metallic materials. Fatigue and Fracture of Engineering Materials and Structures, 2014, vol. 37, no. 9, pp. 958–976. doi: 10.1111/ffe.12158.
- Fleck N.A., Kang K.J., Ashby M.F. Overview no. 112: The cyclic properties of engineering materials. Acta Metallurgica et Materialia, 1994, vol. 42, no. 2, pp. 365–381. doi: 10.1016/0956-7151(94)90493-6.
- Maisuradze M.V., Ryzhkov M.A. Thermal Stabilization of Austenite During Quenching and Partitioning of Austenite for Automotive Steels. Metallurgist, 2018, vol. 62, pp. 337–347. doi: 10.1007/s11015-018-0666-2.
- Speer J.G., De Moor E., Clarke A.J. Critical Assessment 7: Quenching and partitioning. Materials Science and Technology, 2015, vol. 31, no. 1, pp. 3–9. doi: 10.1179/1743284714Y.0000000628.
- Maisuradze M.V., Ryzhkov M.A., Yudin Yu.V., Kuklina A.A. Transformations of supercooled austenite in a promising high-strength steel grade under continuous cooling conditions. Metal Science and Heat Treatment, 2017, vol. 59, pp. 486–490. doi: 10.1007/s11041-017-0176-z.
- Kop T.A., Sietsma J., Van Der Zwaag S. Dilatometric analysis of phase transformations in hypo-eutectoid steels. Journal of Materials Science, 2001, vol. 36, pp. 519–526. doi: 10.1023/A:1004805402404.
- Huang Fei, Chen Qiwei, Ding Hanlin, Wang Yongqiang, Mou Xiuting, Chen Jian. Automotive Steel with a High Product of Strength and Elongation used for Cold and Hot Forming Simultaneously. Materials, 2021, vol. 14, no. 5, article number 1121. doi: 10.3390/ma14051121.
- Yang Feng, Zhou Jian, Han Yun, Liu Peng, Luo Haiwen, Dong Han. A novel cold-rolled medium Mn steel with an ultra-high product of tensile strength and elongation. Materials Letters, 2020, vol. 258, article number 126804. doi: 10.1016/j.matlet.2019.126804.
- Maisuradze M.V., Yudin Yu.V., Kuklina A.A. Formation of Microstructure in Advanced Low-Carbon Steel of Martensitic Class Under Heat Treatment. Metal Science and Heat Treatment, 2021, vol. 62, pp. 550–556. doi: 10.1007/s11041-021-00601-z.
- Maisuradze M.V., Ryzhkov M.A., Lebedev D.I. Microstructure and mechanical properties of martensitic high-strength engineering steel. Metallurgist, 2020, vol. 64, pp. 640–651. doi: 10.1007/s11015-020-01040-6.