THE QUANTITAVE ANALYSIS OF FRACTURE USING THE CONFOCAL LASER SCANNING MICROSCOPY
- Authors: Merson E.D.1, Danilov V.A.1, Merson D.L.1
-
Affiliations:
- Togliatti State University, Togliatti
- Issue: No 4 (2015)
- Pages: 68-75
- Section: Technical Sciences
- URL: https://vektornaukitech.ru/jour/article/view/348
- DOI: https://doi.org/10.18323/2073-5073-2015-4-68-75
- ID: 348
Cite item
Full Text
Abstract
The study of the parts fracture surface is the basic and important part of determination of the fracture process causes and chronology. The quality and objectivity of fractographic analysis depends largely on the effectiveness of tools used for the fracture study. The main disadvantage of traditional methods used in this area is the two-dimensionality of images that greatly complicates the quantitative analysis of the fracture surface. In this context, the method of confocal laser scanning microscopy (CLSM) is one of the prospective techniques providing a high-quality measuring accuracy of the objects surface geometry in three-dimensional space, a wide scanning range along the vertical axis and the necessary depth of field. Moreover, CLSM method does not require the electrical conductivity and special specimen surface preparation, as well as the presence of vacuum.
In this study, the authors developed and tested the technique of exposure and further impact specimen fractures analysis using the CLSM. To be the subject of research, the authors selected the fractures of fully brittle and fully ductile fracture surfaces of 20 grade steel, the fractures of which were obtained during impact tests of the specimens hold at the temperatures of -196°C and +150°C, respectively. During the research, the optimal amplification, the lens type, the scanning pitch and the image noise filter were determined. The research showed that to measure the fracture surface ductility it is possible to use such parameter as the characteristic fracture surface area Sr, which value changes significantly while going from ductile to brittle fracture. The research showed that the CLSM application allows converting the qualitative analysis of metal products fracture into quantitative one improving the objectivity and accuracy of fractographic analysis.
About the authors
Evgeny Dmitrievich Merson
Togliatti State University, Togliatti
Author for correspondence.
Email: mersoned@gmail.com
postgraduate student
Russian FederationVladimir Alekseevich Danilov
Togliatti State University, Togliatti
Email: v.dani1ov@yandex.ru
graduate student
Russian FederationDmitriy Lvovich Merson
Togliatti State University, Togliatti
Email: D.Merson@tltsu.ru
Doctor of Sciences (Physics and Mathematics), Professor
Russian FederationReferences
- Klevtsov G.V., Botvina L.P., Klevtsova N.A., Limar L.V. Fraktodiagnostika razrusheniya metallicheskikh materialov i konstruktsiy [Fractodiagnostics of Fracture of Metallic Materials and Structures]. Moscow, MISiS Publ., 2007. 264 p.
- Balter M.A., Lyubchenko A.P., Aksenova S.I. Fraktografiya – sredstvo diagnostiki razrushennykh detaley [Fractography is a tool for the damaged parts diagnostics]. Moscow, Mashinostroenie Publ., 1978. 184 p.
- Kudrya A.V. The role of structures of different size in plasticity and toughness of structurally inhomogeneous steel. Metallovedenie i termicheskaya obrabotka metallov, 2005, no. 5, pp. 18–23.
- Kudrya A.V., Sokolovskaya E.A. Non-uniformity of different scaled structures and fracture boughness of structurla steels. Izvestiya Rossiyskoy Akademii nauk. Seriya fizicheskaya, 2004, vol. 68, no. 10, pp. 1495–1502.
- Kudrya A.V., Markov E.A. Quantitative evaluation of destruction according to the acoustic emission in various scale measurements. Materialovedenie, 2007, no. 1, pp. 13–18.
- Kudrya A.V., Shtremel M.A. Reliability of data analysis in quality control. Metallovedenie i termicheskaya obrabotka metallov, 2010, no. 7, pp. 50–55.
- Kudrya A.V., Sokolovskaya E.A. Information technologies in quality assurance of metal products. Elektrometallurgiya, 2010, no. 12, pp. 35–43.
- Kudrya A.V., Sokolovskaya E.A., Arsenkin A.M. Effectiveness of using watch facilities of various dimensions to analyze the fracture morphology of upgraded steels. Deformatsiya i razrushenie materialov, 2010, no. 1, pp. 38–44.
- Sokolovskaya E.A. On the results reproducibility of structures and fractures measurements using computerized procedures. Voprosy materialovedeniya, 2013, no. 4, pp. 143–153.
- Kudrya A.V., Sokolovskaya E.A., Trachenko V.A., Le Hai Ning, Skorodumov S.V., Papina K.B. Measurement of nonuniformity of fracture in structural steels with heterogeneous structure. Metallovedenie i termicheskaya obrabotka metallov, 2015, no. 4, pp. 12–18.
- Beachem C.D., Pelloux R.M.N. Electron Fractography – A Tool for the Study of Micromechanisms of Fracturing Processes. Fracture Toughness Testing and its Applications. Chicago, 1965, pp. 210–244.
- Tata B.V.R., Raj B. Confocal laser scanning microscopy: Applications in material science and technology. Bull. Mater. Sci. Springer India, 1998, vol. 21, no. 4, pp. 263–278.
- Hovis D.B., Heuer A.H. The use of laser scanning confocal microscopy (LSCM) in materials science. J. Microsc., 2010, vol. 240, no. 3, pp. 173–180.
- Skálová L., Staňková H., Mašek B. Possible Application of Laser Scanning Confocal Microscopy in Material Science. 8th Multinatl. Congr. Microsc., 2007, pp. 199.
- Iskhodzhanova I.V., Orlov M.R., Grigorenko V.B., Lapteva M.A. Application of the confocal laser imaging microscopy method for corrosive damages study. Trudy VIAM, 2015, no. 4, p. 11.
- Wendt U., Stiebe-Lange K., Smid M., Tonnies K. Quantification of Fracture Surface Topographies based on Confocal Laser Scanning Microscopy. Microscopy and Microanalysis, 2003, vol. 9, pp. 370–371.
- Staňková H., Skálová L., Jacková K., Mašek B. Utilisation of laser confocal microscope Olympus LEXT for the analysis of the fracture area of fine grain steel. Focus on Microscopy 2007. Valencia, 2007, p. 144.
- López-Cepero J.M., Arellano-López A.R. de, Quispe-Cancapa J.J., Martinez-Fernandez J. Confocal Microscopy for Fractographical Surface Characterization of Ceramics. Microscopy and Analysis, 2005, no. 9, pp. 13–15.
- Orlov M.R., Ospennikova O.G., Naprienko S.A., Morozova L.V. Research of fatigue failure of conic gear wheels of reducer of the central drive of the gas turbine engine, made of steel 20X3MVF. Deformatsiya i razrushenie materialov, 2014, no. 7, pp. 18–26.
- Udupa G., Singaperumal M., Sirohi M., Kothiyal M.P. Characterization of surface topography by confocal microscopy: I. Principles and the measurement system. Measurement Science and Technology, 2000, vol. 11, no. 3, pp. 305–314.