THE DEVELOPMENT AND APPLICATION OF THE PROCESS OF PRELIMINARY FORMATION OF THE HIGH-HOMOGENEOUS DRY MIXTURE “ALUMINUM POWDER - SINGLE-WALL CNT” IN THE TECHNOLOGY OF PRODUCTION OF THE ALUMINIUM MATRIX COMPOSITES


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Abstract

The paper considers the problem of synthesis of nanocomposites based on the aluminum matrices reinforced with carbon nanotubes with the high physico-mechanical properties, as related to the achievement of a homogeneous dispersion of carbon nanotubes in the aluminum matrix of a composite. The authors developed the principles of the technology of preparation and determined the requirements for the parameters of the so-called normalized charge (a highly homogeneous dry mixture “aluminum powder - single-wall carbon nanotubes”) intended for the efficient synthesis of composite granules by the mechanical alloying.
Aluminum primary dispersed powder PAD-1 and the single-wall carbon nanotubes TUBALL were used as the raw materials, and the stearic acid was used as a process control agent. The processes of normalization and mechanical alloying were carried out in the mechanical reactor of the author's design. The derived composite pellets were exposed to cold and then to hot compaction. The paper shows the effectiveness of the new approach proposed by the authors to the implementation of effective reinforcement of the aluminum matrix powder by the nanotubes. This approach is based on the provision of effective dispersion of carbon nanotubes into alloyed matrix material by introducing the special technological operation -“normalization” of charge - in the technology of synthesis of composite granules, which are the semi-finished material for the production of a composite material with the high physical and technical characteristics.
The paper presents data on the strength parameters of the semi-finished aluminum matrix composites, which were produced using a normalized charge. It is shown that the application of the developed technology for charge normalization provides the increase in the strength characteristics of semi-finished composite materials by at least 25 % compared with the technologies without the application of normalization. The results obtained during the research can be used when improving the technologies of production of the aluminum matrix composites.

About the authors

N. I. Vetkasov

Ulyanovsk State Technical University

Author for correspondence.
Email: nppwt@ulstu.ru

Vetkasov Nikolai Ivanovich - Doctor of Sciences (Engineering), professor of Chair “Mechanical Engineering”.
432027, Ulyanovsk, Severny Venets Street, 32. Tel.: (8422) 41-82-47

Russian Federation

A. I. Kapustin

Ulyanovsk State Technical University

Email: antak1949@mail.ru

Kapustin Anatoly Ivanovich - Head of Laboratory.
432027, Ulyanovsk, Severny Venets Street, 32. Tel.: (8422) 77-81-03

Russian Federation

V. V. Sapunov

Ulyanovsk State Technical University

Email: sapunov_vv@mail.ru

Sapunov Valery Viktorovich - PhD (Engineering), assistant professor of Chair “Mechanical Engineering”.
432027, Ulyanovsk, Severny Venets Street, 32. Tel.: (8422) 41-80-16

Russian Federation

References

  1. Anantha Prasad M.G., Bandekar N. Study of Microstructure and Mechanical Behavior of Aluminum/Garnet/Carbon Hybrid Metal Matrix Composites (HMMCs) Fabricated by Chill Casting Method. Journal of Materials Science and Chemical Engineering, 2015, vol. 3, no. 3, pp. 1-8.
  2. Gusev A.I. Nanomaterialy, nanostruktury, nanotekhnologii [Nanomaterials, nanostructures, nanotechnologies]. Moscow, Fizmatlit Publ., 2007. 416 p.
  3. Ostovan F., Matori K.A., Toozandehjani M., Oskoueian A., Yusoff H.M., Yunus R., Ariff A.M., Quah H.J., Lim W.F. Effects of CNTs content and milling time on mechanical behavior of MWCNT-reinforced aluminum nanocomposites. Materials Chemistry and Physics, 2015, vol. 166, p. 160-166.
  4. Bunakov N.A., Golovanov V.N., Kozlov D.V., Potapov S.N., Klimov E.S. Obtaining a composite material of aluminum and carbon nanotubes by powder metallurgy method. Sbornik materialov mezhdunarodnogo nauchnogo e-simpoziuma “Fiziko-matematicheskie metody i informatsionnye tekhnologii v estestvoznanii, tekhnike i gumanitarnykh naukakh. Kirov, MTsNIP Publ., 2015, pp. 25-37.
  5. Raviathul B.M., Srivastava V.C., Mukhopadhyay N.K. Microstructural characteristics and mechanical properties of carbon nanotube reinforced aluminum alloy composites produced by ball milling. Materials & Design, 2014, vol. 64, pp. 542-549.
  6. Ci L., Ryu Z., Jin P.N.Y., Ruhle M. Investigation of the interfacial reaction between multi-walled carbon nanotubes and aluminum. Acta Materialia, 2006, vol. 54, no. 20, pp. 5367-5375.
  7. Choi H., Shin J., Min B., Park J., Bae D. Reinforcing effects of carbon nanotubes in structural aluminum matrix nanocomposites. Journal of Materials Research, 2011, vol. 24, no. 8, pp. 2610-2616.
  8. Yang C., Zong Y., Zheng Z., Shan D. Experimental and theoretical investigation on the compressive behavior of aluminum borate whisker reinforced 2024Al composites. Materials Characterization, 2014, vol. 96, pp. 84-92.
  9. Hassan M.T.Z., Esawi A.M.K., Metwalli S. Effect of carbon nanotube damage on the mechanical properties of aluminum-carbon nanotube composites. Journal of Alloys and Compounds, 2014, vol. 607, pp. 215-222.
  10. Yoo S.J., Han S.H., Kim W.J. Strength and strain hardening of aluminum matrix composites with randomly dispersed nanometer-length fragmented carbon nanotubes. Scripta Materialia, 2013, vol. 68, no. 9, pp. 711714.
  11. Wang L., Choi H., Myoung J.M., Lee W. Mechanical alloying of multi-walled carbon nanotubes and aluminium powders for the preparation of carbon/metal composites. Carbon, 2009, vol. 47, no. 15, pp. 3427-3433.
  12. Zhu X., Zhao Y.G., Wu M., Wang H.Y., Jiang Q.C. Effect of Initial Aluminum Alloy Particle Size on the Damage of Carbon Nanotubes during Ball Milling. Materials, 2016, vol. 9, no. 3, pp. 3-18.
  13. Nayan N., Murty S.V.S.N., Sharma S.C., Kumar K.S., Sinha P.P. Calorimetric study on mechanically milled aluminum and multiwall carbon nanotube composites. Materials Characterization, 2011, vol. 62, no. 11, pp. 1087-1093.
  14. Kukovecz A., Kanyo T., Konya Z., Kiricsi I. Long-time low-impact ball milling of multi-wall carbon nanotubes. Carbon, 2005, vol. 43, no. 5, pp. 994 - 1000.
  15. Nam H.R., Kim Y.J., Yang S.S., Ahn J.H. Ball-Milling of Graphite and Multi-Wall Carbon Nanotubes. Journal of Nanoscience and Nanotechnology, 2014, vol. 14, no. 12, pp. 9103-9107.
  16. Narayanan S.S., Manickavasaham G., Moorthy S. Experimental Investigation of Aluminium alloy with MWCNT Composite to increase the technical Properties by Stir Casting Method. IOSR Journal of Mechanical and Civil Engineering, 2015, vol. 12, no. 4 (II), pp. 30-34.
  17. Vetkasov N.I., Kapustin A.I., Sapunov V.V. The formation of phase composition, structural parameters and physical-mechanical properties of composite granules in the process of mechanical alloying of aluminium allotropic forms of carbon. Izvestiya Volgogradskogo gosudarstvennogo tekhnicheskogo universiteta, 2017, no. 12, pp. 7-11.
  18. Vetkasov N.I., Kapustin A.I., Sapunov V.V. The study of the process of mechanical alloying of aluminum by nano-dimensional allotropic modifications of carbon. Vektor nauki Tolyattinskogo gosudarstvennogo universiteta, 2017, no. 3, pp. 24-34.
  19. Lopatina Yu.A., Kurganova Yu.A. Analysis of the hardness measurement of composite materials of the A1 + SiC system. III mezhdunarodnaya nauchnaya shkola molodezhi “Materialovedenie i metallofizika legkikh splavov”. Ekaterinburg, UrFU Publ., 2014, pp. 76-80.
  20. Vetkasov N.I., Kapustin A.I., Sapunov V.V. Experimental study of the process of mechanical alloying of aluminum by technical carbon. Sbornik statey Mezhdunarodnoy nauchno-prakticheskoy konferentsii “Teoreticheskie i prakticheskie aspekty razvitiya nauchnoy mysli v sovremennom mire”. Ufa, AETERNA Publ., 2017, part 2, pp. 18-21.
  21. Gigiberiya V.A., Ar'ev I.A., Lebovka N.I. The stability of suspensions of multiwalled carbon nanotubes in organic solvents in the presence of Triton X-165. Colloid journal, 2012, vol. 74, no. 6, pp. 663-667.

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