Effect of Cold Rolling Reduction on Precipitation of Al20Cu2Mn3 Particles in Al-Cu-Mn System Alloys

Cover Page

Cite item

Abstract

Abstract: Problem. The influence of the degree of cold deformation on the morphology and precipitation of T-phase particles (Al20Cu2Mn3) in Al–Cu–Mn system alloys (ALTEK) during final annealing has been insufficiently studied. This complicates the prediction of properties and the optimisation of thermomechanical processing of sheets and foils for electrical engineering applications. Objective. To establish the patterns of the influence of the cold rolling deformation degree (50 and 90 %) on the formation, morphology, and size of T-phase (Al20Cu2Mn3) particles, as well as on the complex of mechanical and electrical properties of sheets and foils made of ALTEK alloy of the Al–2%Cu–2%Mn system, produced by the following scheme: hot rolling → cold rolling → annealing at 400 C. Methods. Ingots were produced by chill casting and subjected to hot rolling, intermediate annealing, and cold rolling. A portion of the specimens was annealed at 400 °С for 3 hours. The microstructure was studied using transmission electron microscopy. Electrical conductivity (EC) and mechanical properties were measured. Results. It was found that the majority of Al20Cu2Mn3 particles is formed during hot rolling. Cold deformation causes dislocation hardening and fragmentation of existing particles. Regardless of the degree of deformation (50 or 90 %), annealing at 400 °С forms an identical microstructure with lamellar T-phase precipitates measuring 120–200 nm. The electrical conductivity increases from 14.6–14.8 MS/m to 29.6 MS/m after annealing. Conclusions. The degree of cold deformation in the investigated range does not affect the volume fraction of T-phase particles after annealing. The main increase in electrical conductivity and softening are caused by a reduction in dislocation density and further decomposition of the solid solution with coagulation of particles formed during the hot rolling stage.

About the authors

Vyacheslav Yu. Chinov

Siberian state industrial university

Author for correspondence.
Email: chinov_vy@sibsiu.ru
ORCID iD: 0009-0004-6874-0870

postgraduate student of Professor V.M. Finkel Chair of natural sciences, lecturer at the Chair of metal forming and materials science of EVRAZ ZSMK (West Siberian Metallurgical Complex)

Russian Federation, 654007, Russia, Novokuznetsk, Kirov Street, 42.

Alina A. Levagina

Siberian state industrial university

Email: levagina_aa@sibsiu.ru
ORCID iD: 0000-0002-7270-6008

master, leading engineer at the Chair of metal forming and materials science of EVRAZ ZSMK (West Siberian Metallurgical Complex)

Russian Federation, 654007, Russia, Novokuznetsk, Kirov Street, 42.

Evgeny V. Aryshensky

Siberian state industrial university

Email: ar-evgenii@yandex.ru
ORCID iD: 0000-0001-6869-4764

Doctor of Sciences (Engineering), Associate Professor, Head of Chair of metal forming and materials science of EVRAZ ZSMK
(West Siberian Metallurgical Complex)

Russian Federation, 654007, Russia, Novokuznetsk, Kirov Street, 42.

Dmitry Yu. Rasposienko

M.N. Mikheev Institute of metal physics of the Ural branch of RAS

Email: rasposienko@imp.uran.ru
ORCID iD: 0000-0002-7670-9054

PhD (Engineering), Head of the laboratory of non-ferrous alloys. 

Russian Federation, 620108, Russia, Yekaterinburg, Sofya Kovalevskaya Street, 18.

Sergey V. Konovalov

Siberian state industrial university

Email: konovalov@sibsiu.ru
ORCID iD: 0000-0003-4809-8660

Doctor of Sciences (Engineering), Professor, vice-rector for research and innovation. 

Russian Federation, 654007, Russia, Novokuznetsk, Kirov Street, 42.

References

  1. Abnar B., Gashtiazar S., Rometsch P., Javidani M. Advanced thermal-resistant aluminum conductor alloys: A comprehensive review. International Journal of Minerals, Metallurgy and Materials, 2026, vol. 33, no. 1, pp. 68–93. doi: 10.1007/s12613-025-3265-9.
  2. Levagina A.A., Aryshenskiy E.V., Konovalov S.V., Drits A.M., Tepterev M.S. Studies of microstructure and properties formation during production of Al-2Cu-2Mn alloy strip. Polzunovskiy vestnik, 2025, no. 1, pp. 187–196. doi: 10.25712/ASTU.2072-8921.2025.01.023.
  3. Levagina A.A., Aryshenskiy E.V., Konovalov S.V., Korotkova N.O., Tepterev M.S., Borminskiy S.A. Mechanical and electrical properties of altek alloy electrical foil for transformer windings. Vestnik of Samara University. Aerospace and Mechanical Engineering, 2025, vol. 24, no. 1, pp. 143–152. doi: 10.18287/2541-7533-2025-24-1-143-152.
  4. Rogachev S.O., Tsydenov K.A., Andreev V.A., Bondareva S.A. Effect of Rotary Forging on the Microstructure and Mechanical Properties of Al – Cu – Mn Alloys Used in Electrical Engineering. Metal Science and Heat Treatment, 2025, vol. 67, pp. 376–382. doi: 10.1007/s11041-025-01172-z.
  5. Xiao Duan, Fulin Wen, Qin Yang, Dengzhi Zheng, Jianhui Liu, Mengwu Wu. Effect of Al–Ti–C–B–RE refiner on the microstructure and mechanical properties of Al–Cu–Mn alloy. Journal of Materials Research, 2025, vol. 40, no. 23, pp. 3377–3390. doi: 10.1557/s43578-025-01742-0.
  6. Korotkova N.O., Shurkin P.K., Cherkasov S.O., Aksenov A.A., Finogeev A.S. Effect of copper concentration and annealing temperature on the structure and mechanical properties of Al-2Wt.%mn ingots and cold rolled sheets. Izvestiya. Non-ferrous Metallurgy, 2022, vol. 28, no. 1, pp. 67–78. doi: 10.17073/0021-3438-2022-1-67-78.
  7. Yujie Lin, Mingdong Wu, Daihong Xiao, Yunzhu Ma, Wensheng Liu. Effect of minor La addition on the microstructure and mechanical properties of cast Al-Cu-Mn alloys. Journal of Alloys and Compounds, 2025, vol. 1021, article number 179747. doi: 10.1016/j.jallcom.2025.179747.
  8. Ruofei Zhu, Weidong Chen, Zhu Chen, Yi Sui, Yinhui Qu. Effect of combined addition of Ni and Sc on microstructure and high-temperature mechanical properties of an Al-Cu-Mn alloy. Journal of Alloys and Compounds, 2025, vol. 1023, article number 179971. doi: 10.1016/j.jallcom.2025.179971.
  9. Na Yang, Meigui Ou, Yu Liang. The Effect of Aging Temperature on the Mechanical Properties and Corrosion Behavior of Al-Cu-Mn Alloy. Journal of Alloys and Compounds, 2025, vol. 1050, article number 185694. doi: 10.1016/j.jallcom.2025.185694.
  10. Petrova A.N., Rasposienko D.Y., Astafyev V.V., Yakovleva A.O. Structure and strength of Al-Mn-Cu-Zr-Cr-Fe ALTEC alloy after radial-shear rolling. Letters on Materials, 2023, vol. 13, no. 2, pp. 177–182. doi: 10.22226/2410-3535-2023-2-177-182.
  11. Belov N.A., Korotkova N.O., Akopyan T.K., Pesin A.M. Phase composition and mechanical properties of Al–1.5% Cu–1.5% Mn–0.35% Zr (Fe, Si) wire alloy. Journal of Alloys and Compouёnds, 2019, vol. 782, pp. 735–746. doi: 10.1016/j.jallcom.2018.12.240.
  12. Xu-Dong Ma, Dan Zhang, Bai-Xin Dong, Hong-Yu Yang, Shi-Li Shu, Liang-Yu Chen, Fan Zhang, Jie Kang, Jia Meng, Cheng-Gang Wang, Kuang Cao, Jian Qiao, Feng Qiu, Qi-Chuan Jiang. Enhancing high-temperature performance of Al—Cu alloys via nanoceramic particle-induced grain boundary stabilization and precipitate manipulation. Materials Characterization, 2025, vol. 229, part B, article number 115628. doi: 10.1016/j.matchar.2025.115628.
  13. Belov N.A., Cherkasov S.O., Korotkova N.O., Tsydenov K.A. Processability and structural evolution of round ingots of Al - 2 % Cu - 2 % Mn alloy during forming. Tsvetnye Metally, 2023, no. 1, pp. 77–82. doi: 10.17580/tsm.2023.01.10.
  14. Qilei Li, Guangjie Huang, Yu Cao, Zhihong Jia, Jie He, Ziman Liang, Qing Liu. Enhancement in dispersoid precipitation and dispersion strengthening by prior deformation in an Al–Mg–Mn alloy. Materials Science and Engineering: A, 2023, vol. 869, article number 144808. doi: 10.1016/j.msea.2023.144808.
  15. Youfang Cao, Longtao Jiang, Guwei Shen, Deng Gong, Jiancun Rao, Guoqin Chen. Quantitative study on the microstructural evolution and dimensional stability mechanism of 2024 Al alloy during long-term thermal cycling. Journal of Materials Research and Technology, 2024, vol. 28, pp. 2313–2325. doi: 10.1016/j.jmrt.2023.12.134.
  16. Bignon M., Ziyu Ma, Robson J.D., Shanthraj P. Interactions between plastic deformation and precipitation in Aluminium alloys: A crystal plasticity model. Acta Materialia, 2023, vol. 247, article number 118735. doi: 10.1016/j.actamat.2023.118735.
  17. Eymann M., Perez M., Chaise T., Elguedj T., Geslin P.-A. A full-field approach for precipitation in metallic alloys. Comparison with a mean-field model. Acta Materialia, 2024, vol. 279, article number 120296. doi: 10.1016/j.actamat.2024.120296.
  18. Han Zhang, Yanqing Xue, Yadong Lv, Qitang Hao, Ruirun Chen, Wentao Yu, Haiyan Yang, Yanmin Zhang. Novel thermomechanical processing of Al-Cu-Mn-Mg-Ag alloy for enhanced strength-ductility performance. Journal of Materials Science & Technology, 2026, vol. 250, pp. 108–122. doi: 10.1016/j.jmst.2025.06.030.

Supplementary files

Supplementary Files
Action
1. JATS XML

Copyright (c) 2026 Chinov V.Y., Levagina A.A., Aryshensky E.V., Rasposienko D.Y., Konovalov S.V.

Creative Commons License
This work is licensed under a Creative Commons Attribution 4.0 International License.