Mechanical properties of nitrogen-containing austenitic steel obtained by multilayer arc deposition of a flux-cored wire
- Authors: Soboleva N.N.1, Kuznetsov A.M.1, Mushnikov A.N.1, Veselova V.E.2, Smolentsev A.S.1
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Affiliations:
- Institute of Engineering Science of the Ural Branch of RAS
- 620049, Россия, г. Екатеринбург, ул. Комсомольская, 34.
- Issue: No 1 (2026)
- Pages: 83-95
- Section: Articles
- URL: https://vektornaukitech.ru/jour/article/view/1185
- DOI: https://doi.org/10.18323/2782-4039-2026-1-75-7
- ID: 1185
Cite item
Abstract
Austenitic stainless steels are characterized by paramagnetic properties, good ductility, toughness and corrosion resistance. However, their strength properties are relatively low. Nitrogen alloying is an effective way to increase their strength. The increased nitrogen and manganese content in steels of this class makes it possible to reduce the nickel content. The presence of delta ferrite in the structure of austenitic steels can improve their resistance to the formation of hot cracks. Wire arc additive manufacturing is a modern method of producing parts from austenitic steels. The authors have developed a flux-cored wire for wire arc additive manufacturing, which makes it possible to deposit metal containing nitrogen in chemical composition, high chromium and manganese content, low nickel content, and providing a structure of austenite and a small amount of δ-ferrite. The aim of the work was to certify the deposited material, including t he determination of structural features, micromechanical characteristics, and mechanical properties under conditions of static tensile loading and cyclic loading in the low cycle fatigue testing. As a result of multilayer depositing, deposited layers were obtained with a composition (by wt. %): < 0.1 C; 21.1 Cr; 3.3 Ni; 5.0 Mn; 2.0 Mo; 2.8 Cu; 0.239 N. According to the results of X-ray and EBSD analyses, the structure of the deposited layers consists of austenite and 6 wt. % δ-ferrite. The properties of the studied material are compared with those of the widely used austenitic stainless steel AISI 321. Higher strength properties of the studied material are shown both during instrumental microindentation (HM=2.7 GPa; HIT=3.1 GPa) and static tensile testing (σ0,2=595 MPa; σВ=790 MPa; δ=28 %). The transition to multi-cycle fatigue of the developed material occurs at a stress amplitude within 550 MPa.
About the authors
Natalia N. Soboleva
Institute of Engineering Science of the Ural Branch of RAS
Author for correspondence.
Email: soboleva@imach.uran.ru
ORCID iD: 0000-0002-7598-2980
PhD (Engineering),
Head of sector.
Alexander M. Kuznetsov
Institute of Engineering Science of the Ural Branch of RAS
Email: starkraft.01@mail.ru
ORCID iD: 0009-0000-5310-0257
research assistant
Russian Federation, 620049, Russia, Yekaterinburg, Komsomolskaya Street, 34.Aleksandr N. Mushnikov
Institute of Engineering Science of the Ural Branch of RAS
Email: mushnikov@imach.uran.ru
ORCID iD: 0000-0001-7073-6476
PhD (Engineering),
Head of laboratory.
Valeria E. Veselova
620049, Россия, г. Екатеринбург, ул. Комсомольская, 34.
Email: veselova@imach.uran.ru
ORCID iD: 0000-0002-4955-6435
PhD (Engineering), researcher.
Russian Federation, 620049, Russia, Yekaterinburg, Komsomolskaya Street, 34.Alexey S. Smolentsev
Institute of Engineering Science of the Ural Branch of RAS
Email: a.s.smolentsev@mail.ru
ORCID iD: 0009-0002-0572-0384
researcher.
Russian Federation, 620049, Russia, Yekaterinburg, Komsomolskaya Street, 34.References
- Kvackaj T., Bidulská J., Fedoríková A., Bidulský R. Mechanical Properties and Strengthening Contributions of AISI 316 LN Austenitic Stainless Steel Grade. Materials, 2025, vol. 18, no. 3, article number 499. doi: 10.3390/ma18030499.
- Pixner F., Arnoldt A., Unger M., Schneider-Broskamp C., Bharadwaj K., Mayrhofer F., Gradinger R., Klein T. On the viability of in-situ alloying via process gas mixtures in wire arc directed energy deposition of austenitic stainless steel. Journal of Materials Processing Technology, 2025, vol. 337, article number 118738. doi: 10.1016/j.jmatprotec.2025.118738.
- Wang Yong, Wang Zhenhua, Wang Wei, Ma Bingyang. Effect of nitrogen content on mechanical properties of 316L(N) austenitic stainless steel. Materials Science and Engineering: A, 2023, vol. 884, article number 145549. doi: 10.1016/j.msea.2023.145549.
- Cui Chengsong, Uhlenwinkel V., Schulz A., Zoch H.W. Austenitic stainless steel powders with increased nitrogen content for laser additive manufacturing. Metals, 2020, vol. 10, no. 1, article number 61. doi: 10.3390/met10010061.
- Kazakov A.A., Oryshchenko A.S., Fomina O.V., Zhitenev A.I., Vikhareva T.V. Controlling behavior of δ-ferrite in nitrogen-containing chromium–nickel–manganese steels. Inorganic Materials: Applied Research, 2017, vol. 8, no. 6, pp. 817–826. doi: 10.1134/S2075113317060077.
- Padilha A.F., Rios P.R. Decomposition of austenite in austenitic stainless steels. ISIJ International, 2002, vol. 42, no. 4, pp. 325–337. doi: 10.2355/isijinternational.42.325.
- Osoba L.O., Elemuren R.A., Ekpe I.C. Influence of delta ferrite on corrosion susceptibility of AISI 304 austenitic stainless steel. Cogent Engineering, 2016, vol. 3, no. 1, pp. 1–8. doi: 10.1080/23311916.2016.1150546.
- Queguineur A., Asadi R., Ostolaza M., Valente E.H., Nadimpalli V.K., Mohanty G., Hascoët J.-Y., Ituarte I.F. Wire arc additive manufacturing of thin and thick walls made of duplex stainless steel. The International Journal of Advanced Manufacturing Technology, 2023, vol. 127, no. 1-2, pp. 381–400. doi: 10.1007/s00170-023-11560-5.
- Jin Wanwan, Zhang Chaoqun, Jin Shuoya, Tian Yingtao, Wellmann D., Liu Wen. Wire arc additive manufacturing of stainless steels: A review. Applied Sciences (Switzerland), 2020, vol. 10, no. 5, pp. 270–286. doi: 10.3390/app10051563.
- Zhang Yiqi, Wu Shaojie, Cheng Fangjie. A duplex stainless steel (DSS) with striking tensile strength and corrosion resistance produced through wire arc-additive manufacturing (WAAM) using a newly developed flux-cored wire. Materials Letters, 2022, vol. 313, article number 131760. doi: 10.1016/j.matlet.2022.131760.
- Savrai R.A., Skorynina P.A., Makarov A.V., Osintseva A.L. Effect of Liquid Carburizing at Lowered Temperature on the Micromechanical Characteristics of Metastable Austenitic Steel. Physics of Metals and Metallography, 2020, vol. 121, no. 10, pp. 1015–1020. doi: 10.1134/S0031918X20100105.
- Soboleva N.N., Davydova N.A., Makarov A.V. The effect of the multiplicity of frictional action on the micromechanical properties of NiCrBSi-coatings. Diagnostics, Resource and Mechanics of materials and structures, 2022, no. 5, pp. 50–59. doi: 10.17804/2410-9908.2022.5.050-059.
- Kannan A.R., Shanmugam N.S., Sanjeeviprakash K., Palguna Y., Korla R., Lee Wonjoo, Jeong Yu Hyeong, Yoon Jonghun. Room and high-temperature tensile properties of austenitic stainless steel 321 fabricated by wire arc additive manufacturing. Journal of Materials Research and Technology, 2025, vol. 36, pp. 3996–4004. doi: 10.1016/j.jmrt.2025.04.084.
- Mantserov S.A., Anosov M.S., Mordovina Yu.S., Chernigin M.A. Effect of 3D printing mode on structure and fatigue strength of 30CrMnSi steel. Izvestiya vuzov. Chernaya metallurgiya, 2024, vol. 67, no. 6, pp. 696–701. doi: 10.17073/0368-0797-2024-6-696-701.
- Queguineur A., Cherukuri R., Lambai A., Dalal M.S., Peura P., Mohanty G., Hascoët J.-Y., Ituarte I.F. Correlated high throughput nanoindentation mapping and microstructural characterization of wire and arc additively manufactured 2205 duplex stainless steel. Welding in the World, 2024, vol. 68, pp. 2247–2257. doi: 10.1007/s40194-024-01795-5.
- Speidel M.O. New nitrogen-bearing austenitic stainless steels with high strength and ductility. Metal Science and Heat Treatment, 2005, vol. 47, no. 11-12, pp. 489–493. doi: 10.1007/s11041-006-0017-y.
- Naizabekov A., Arbuz A., Lezhnev S., Panin E., Knapinski M. Study of Technology for Ultrafine-Grained Materials for Usage as Materials in Nuclear Power. New Trends in Production Engineering, 2019, vol. 2, no. 2, pp. 114–125. doi: 10.2478/ntpe-2019-0077.
- Kumar S.M., Sasikumar R., Kannan A.R., Pramod R., Kumar N.P., Shanmugam N.S., Vishnukumar M. Microstructural administered mechanical properties and corrosion behaviour of wire plus arc additive manufactured SS 321 plate. Proceedings of the Institution of Mechanical Engineers, Part C: Journal of Mechanical Engineering Science, 2021, vol. 235, no. 24, pp. 7627–7633. doi: 10.1177/09544062211042039.
- Khorrami M., Hanzaki A.Z., Abedi H.R., Mola J., Chen Guanghui, Minarik P. Temperature dependence of tensile deformation behavior and strain hardening of lean duplex stainless steels. Journal of Materials Research and Technology, 2022, vol. 20, pp. 330–342. doi: 10.1016/j.jmrt.2022.07.040.
- Zheng Chengsi, Yu Wangwei. Effect of low-temperature on mechanical behavior for an AISI 304 austenitic stainless steel. Materials Science and Engineering: A, 2018, vol. 710, pp. 359–365. doi: 10.1016/j.msea.2017.11.003.
- Barannikova S.A., Kolosov S.V., Shlyakhova G.V. Influence of Temperature and Deformation on Structure and Mechanical Properties of Stainless Steel. Russian Physics Journal, 2023, vol. 66, no. 1, pp. 38–42. doi: 10.1007/s11182-023-02902-7.
- Botvina L.R., Beletsky E.N., Tyutin M.R., Demina Yu.A., Sinev I.O., Bolotnikov A.I. Fracture of 30crmnsia steel under mixed-mode loads. Physical Mesomechanics, 2023, vol. 26, no. 4, pp. 391–401. doi: 10.1134/s1029959923040021.
- Chang Le, Zhou Bin-Bin, Ma Tian-Hao, Li Jian, He Xiao-Hua, Zhou Chang-Yu. Comparisons of low cycle fatigue behavior of CP-Ti under stress and strain-controlled modes in transverse direction. Materials Science and Engineering: A, 2019, vol. 746, pp. 27–40. doi: 10.1016/j.msea.2018.12.125.
- Li Yajing, Yuan Yutong, Wang Dexin, Fu Sichao, Song Danrong, Vedani M., Chen Xu. Low cycle fatigue behavior of wire arc additive manufactured and solution annealed 308 L stainless steel. Additive Manufacturing, 2022, vol. 52, article number 102688. doi: 10.1016/j.addma.2022.102688.
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